I-Pilot Reactor ye-PX Oxidation yovavanyo oluqhubekayo
Inkqubo esisiseko:
Ukufudumala inkqubo, kwaye uyihlambulule nge-nitrogen de umxholo we-oksijini we-outlet tail gas ube ngu-zero.
Yongeza ukutya okumanzi (i-acetic acid kunye ne-catalyst) kwinkqubo kwaye ngokuqhubekayo ukufudumala inkqubo kwiqondo lokushisa lokuphendula.
Yongeza umoya ococekileyo, qhubeka ufudumeza kude kube ukusabela kubangelwa, kwaye uqale ukugquma.
Xa inqanaba lolwelo lwe-reactants lifikelela kubude obufunekayo, qalisa ukulawula ukukhutshwa, kwaye ulawule isantya sokukhutshwa ukuze ugcine umgangatho we-liquid uzinzile.
Kuyo yonke inkqubo yokusabela, uxinzelelo kwinkqubo ngokusisiseko uzinzile ngenxa yoxinzelelo lwangaphambili kunye nomva-up.
Ngokuqhubeka kwenkqubo yokusabela, kwi-reaction ye-tower, igesi evela phezulu kwinqaba ingena kwi-gas-liquid separator ngokusebenzisa i-condenser kwaye ingena kwi-tank yokugcina izinto.Inokubuyiselwa kwinqaba okanye ikhutshwe kwibhotile yokugcina impahla ngokweemfuno zovavanyo.
Ukuphendula kweketile, igesi evela kwi-kettle cover ingangeniswa kwi-condenser kwi-outlet yenqaba.I-liquid condensed is pumped back to reactor with the constant flux pump, kwaye igesi ingena kwinkqubo yonyango yegesi yomsila.